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5.35U

Introduction to Experimental Chemistry

Undergraduate · Historical course

Fall 2012

Topics

  • Introduction to Electronic Spectroscopy (Experiments 2–4)
  • IR Spectroscopy (Experiments 5–6)
  • IR Spectroscopy of Proteins (Experiment 7)
  • TeachSpin 15 MHz NMR (Experiment 8)
  • NMR, 300 MHz (Experiment 9)
  • Oral Examinations
  • Synthesis of [Co(NNH 3 ) 4 (CO 3 )]NO 3
  • Synthesis of [Co(NNH 3 ) 5 Cl]Cl 2
  • Lambert-Beer study
  • Kinetics Measurements at 60 C
  • Kinetics Measurements at 40 C
  • Kinetics Measurements at 70 C
  • Report Interview
  • Polymer Synthesis
  • Polymer Work-up and Purification
  • GPC Characterization and UV-Vis Characterization
  • Device Fabrication
  • Device measurements
Sources